Novel Approach for Determination of Potentially Toxic Elements via ICP-OES in Aqueous Solutions of Building Materials with Industrial Byproduct Addition
2019
Autori
Mijatović, NevenkaTerzić, Anja
Pezo, Lato
Miličić, Ljiljana
Milosavljević, Aleksandra
Živojinović, Dragana
Članak u časopisu (Objavljena verzija)
Metapodaci
Prikaz svih podataka o dokumentuApstrakt
New global tendencies for waste materials reusing in building materials are imposing the request for improved performances of chemical analysis methods and the improvements of matrices used. A new method for optical emission spectrometry with inductively coupled plasma (ICP-OES) is developed and validated for the chemical analysis (35 elements: Al, Be, Cd, So, Cr, Cu, Fe, Mn, Mo, Ni, V, Mo, Zn, Pb , Bi, Si, Zr, W, As, Se, Sb, Sn, Ti, Ba, B, Ag, Mg, Ca, K, Na, S, P, Ga, In, Li) in leachate of fly ash. Validation performances and the uncertainty of measurement were resolved. Uncertainty of measurements were resolved by three routes: validation procedure, participation in proficiency testing (PT) schemes and standard method. The obtained method is a new simple and effective analyzing route for determination of undesired trace elements and their quantity comprised in leachates of fly ash, and leachates of building materials with addition of fly ash (cement binders and mortars). In order to... prove its accuracy and precision, the developed method was employed on laboratory samples of cement binders and mortars. Results were compared with limit values provided in the standard. Multivariate analyses, i.e. cluster analysis and principal component analysis, were applied to establish interrelations between analyzed samples, and to certify the developed ICP-OES method.
Ključne reči:
Waste materials / Leaching / Building materials / Analytical procedures / Analytical modelingIzvor:
Science of Sintering, 2019, 51, 4, 429-444Izdavač:
- Međunarodni Institut za nauku o sinterovanju, Beograd
Finansiranje / projekti:
- Razvoj i primena multifunkcionalnih materijala na bazi domaćih sirovina modernizacijom tradicionalnih tehnologija (RS-45008)
- Usmerena sinteza, struktura i svojstva multifunkcionalnih materijala (RS-172057)
DOI: 10.2298/SOS1904429M
ISSN: 0350-820X
WoS: 000509869400008
Scopus: 2-s2.0-85078854100
Institucija/grupa
Institut za ispitivanje materijalaTY - JOUR AU - Mijatović, Nevenka AU - Terzić, Anja AU - Pezo, Lato AU - Miličić, Ljiljana AU - Milosavljević, Aleksandra AU - Živojinović, Dragana PY - 2019 UR - http://rims.institutims.rs/handle/123456789/369 AB - New global tendencies for waste materials reusing in building materials are imposing the request for improved performances of chemical analysis methods and the improvements of matrices used. A new method for optical emission spectrometry with inductively coupled plasma (ICP-OES) is developed and validated for the chemical analysis (35 elements: Al, Be, Cd, So, Cr, Cu, Fe, Mn, Mo, Ni, V, Mo, Zn, Pb , Bi, Si, Zr, W, As, Se, Sb, Sn, Ti, Ba, B, Ag, Mg, Ca, K, Na, S, P, Ga, In, Li) in leachate of fly ash. Validation performances and the uncertainty of measurement were resolved. Uncertainty of measurements were resolved by three routes: validation procedure, participation in proficiency testing (PT) schemes and standard method. The obtained method is a new simple and effective analyzing route for determination of undesired trace elements and their quantity comprised in leachates of fly ash, and leachates of building materials with addition of fly ash (cement binders and mortars). In order to prove its accuracy and precision, the developed method was employed on laboratory samples of cement binders and mortars. Results were compared with limit values provided in the standard. Multivariate analyses, i.e. cluster analysis and principal component analysis, were applied to establish interrelations between analyzed samples, and to certify the developed ICP-OES method. PB - Međunarodni Institut za nauku o sinterovanju, Beograd T2 - Science of Sintering T1 - Novel Approach for Determination of Potentially Toxic Elements via ICP-OES in Aqueous Solutions of Building Materials with Industrial Byproduct Addition EP - 444 IS - 4 SP - 429 VL - 51 DO - 10.2298/SOS1904429M ER -
@article{ author = "Mijatović, Nevenka and Terzić, Anja and Pezo, Lato and Miličić, Ljiljana and Milosavljević, Aleksandra and Živojinović, Dragana", year = "2019", abstract = "New global tendencies for waste materials reusing in building materials are imposing the request for improved performances of chemical analysis methods and the improvements of matrices used. A new method for optical emission spectrometry with inductively coupled plasma (ICP-OES) is developed and validated for the chemical analysis (35 elements: Al, Be, Cd, So, Cr, Cu, Fe, Mn, Mo, Ni, V, Mo, Zn, Pb , Bi, Si, Zr, W, As, Se, Sb, Sn, Ti, Ba, B, Ag, Mg, Ca, K, Na, S, P, Ga, In, Li) in leachate of fly ash. Validation performances and the uncertainty of measurement were resolved. Uncertainty of measurements were resolved by three routes: validation procedure, participation in proficiency testing (PT) schemes and standard method. The obtained method is a new simple and effective analyzing route for determination of undesired trace elements and their quantity comprised in leachates of fly ash, and leachates of building materials with addition of fly ash (cement binders and mortars). In order to prove its accuracy and precision, the developed method was employed on laboratory samples of cement binders and mortars. Results were compared with limit values provided in the standard. Multivariate analyses, i.e. cluster analysis and principal component analysis, were applied to establish interrelations between analyzed samples, and to certify the developed ICP-OES method.", publisher = "Međunarodni Institut za nauku o sinterovanju, Beograd", journal = "Science of Sintering", title = "Novel Approach for Determination of Potentially Toxic Elements via ICP-OES in Aqueous Solutions of Building Materials with Industrial Byproduct Addition", pages = "444-429", number = "4", volume = "51", doi = "10.2298/SOS1904429M" }
Mijatović, N., Terzić, A., Pezo, L., Miličić, L., Milosavljević, A.,& Živojinović, D.. (2019). Novel Approach for Determination of Potentially Toxic Elements via ICP-OES in Aqueous Solutions of Building Materials with Industrial Byproduct Addition. in Science of Sintering Međunarodni Institut za nauku o sinterovanju, Beograd., 51(4), 429-444. https://doi.org/10.2298/SOS1904429M
Mijatović N, Terzić A, Pezo L, Miličić L, Milosavljević A, Živojinović D. Novel Approach for Determination of Potentially Toxic Elements via ICP-OES in Aqueous Solutions of Building Materials with Industrial Byproduct Addition. in Science of Sintering. 2019;51(4):429-444. doi:10.2298/SOS1904429M .
Mijatović, Nevenka, Terzić, Anja, Pezo, Lato, Miličić, Ljiljana, Milosavljević, Aleksandra, Živojinović, Dragana, "Novel Approach for Determination of Potentially Toxic Elements via ICP-OES in Aqueous Solutions of Building Materials with Industrial Byproduct Addition" in Science of Sintering, 51, no. 4 (2019):429-444, https://doi.org/10.2298/SOS1904429M . .