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Dehydration investigations of a refractory concrete using DTA method

Authorized Users Only
2012
Authors
Obradović, Nina
Terzić, Anja
Pavlović, Ljubica
Filipović, S.
Pavlović, Vladimir
Article (Published version)
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Abstract
The base mix refractory concrete is corundum-based, containing corundum as refractory aggregate and CAC as hydraulic binder, with a spinel as an additive. The authors investigated the dehydration reactions which occur from the moment when water is added (at the beginning of components mixing), to the moment when installed refractory concrete lining is put into the service. Sintering process kinetic of low-cement content refractory concrete was investigated by means of differential thermal analysis at four different heating rates (5, 10, 20, and 30 A degrees C/min). Thus, temperature was increased from 20 to 1100 A degrees C. It was noticed that first dehydration step occurs at lower temperatures, indicating at a desorption of physically adsorbed and interlayer water molecules. Second dehydration step, at higher temperatures is due to dehydroxylation of the lattices and decomposition of the interlayer anions.
Keywords:
Sintering kinetics / Refractory concrete / DTA
Source:
Journal of Thermal Analysis and Calorimetry, 2012, 110, 1, 37-41
Publisher:
  • Springer, Dordrecht
Funding / projects:
  • Serbian Academy of Sciences and Arts
  • Directed synthesis, structure and properties of multifunctional materials (RS-172057)
  • Development and application of multifunctional materials using domestic raw materials in upgraded processing lines (RS-45008)

DOI: 10.1007/s10973-011-1880-3

ISSN: 1388-6150

WoS: 000309709900005

Scopus: 2-s2.0-84867520176
[ Google Scholar ]
8
6
URI
http://rims.institutims.rs/handle/123456789/158
Collections
  • Radovi istraživača / Researchers' publications
Institution/Community
Institut za ispitivanje materijala
TY  - JOUR
AU  - Obradović, Nina
AU  - Terzić, Anja
AU  - Pavlović, Ljubica
AU  - Filipović, S.
AU  - Pavlović, Vladimir
PY  - 2012
UR  - http://rims.institutims.rs/handle/123456789/158
AB  - The base mix refractory concrete is corundum-based, containing corundum as refractory aggregate and CAC as hydraulic binder, with a spinel as an additive. The authors investigated the dehydration reactions which occur from the moment when water is added (at the beginning of components mixing), to the moment when installed refractory concrete lining is put into the service. Sintering process kinetic of low-cement content refractory concrete was investigated by means of differential thermal analysis at four different heating rates (5, 10, 20, and 30 A degrees C/min). Thus, temperature was increased from 20 to 1100 A degrees C. It was noticed that first dehydration step occurs at lower temperatures, indicating at a desorption of physically adsorbed and interlayer water molecules. Second dehydration step, at higher temperatures is due to dehydroxylation of the lattices and decomposition of the interlayer anions.
PB  - Springer, Dordrecht
T2  - Journal of Thermal Analysis and Calorimetry
T1  - Dehydration investigations of a refractory concrete using DTA method
EP  - 41
IS  - 1
SP  - 37
VL  - 110
DO  - 10.1007/s10973-011-1880-3
ER  - 
@article{
author = "Obradović, Nina and Terzić, Anja and Pavlović, Ljubica and Filipović, S. and Pavlović, Vladimir",
year = "2012",
abstract = "The base mix refractory concrete is corundum-based, containing corundum as refractory aggregate and CAC as hydraulic binder, with a spinel as an additive. The authors investigated the dehydration reactions which occur from the moment when water is added (at the beginning of components mixing), to the moment when installed refractory concrete lining is put into the service. Sintering process kinetic of low-cement content refractory concrete was investigated by means of differential thermal analysis at four different heating rates (5, 10, 20, and 30 A degrees C/min). Thus, temperature was increased from 20 to 1100 A degrees C. It was noticed that first dehydration step occurs at lower temperatures, indicating at a desorption of physically adsorbed and interlayer water molecules. Second dehydration step, at higher temperatures is due to dehydroxylation of the lattices and decomposition of the interlayer anions.",
publisher = "Springer, Dordrecht",
journal = "Journal of Thermal Analysis and Calorimetry",
title = "Dehydration investigations of a refractory concrete using DTA method",
pages = "41-37",
number = "1",
volume = "110",
doi = "10.1007/s10973-011-1880-3"
}
Obradović, N., Terzić, A., Pavlović, L., Filipović, S.,& Pavlović, V.. (2012). Dehydration investigations of a refractory concrete using DTA method. in Journal of Thermal Analysis and Calorimetry
Springer, Dordrecht., 110(1), 37-41.
https://doi.org/10.1007/s10973-011-1880-3
Obradović N, Terzić A, Pavlović L, Filipović S, Pavlović V. Dehydration investigations of a refractory concrete using DTA method. in Journal of Thermal Analysis and Calorimetry. 2012;110(1):37-41.
doi:10.1007/s10973-011-1880-3 .
Obradović, Nina, Terzić, Anja, Pavlović, Ljubica, Filipović, S., Pavlović, Vladimir, "Dehydration investigations of a refractory concrete using DTA method" in Journal of Thermal Analysis and Calorimetry, 110, no. 1 (2012):37-41,
https://doi.org/10.1007/s10973-011-1880-3 . .

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